Sol-gel approach to preparing germanium disulphide

A. B. Seddon, S. N.B. Hodgson, M. G. Scott

    Research output: Contribution to journalArticle

    1 Citation (Scopus)

    Abstract

    A sol-gel route to germanium disulphide reported in the literature, via dihydrogen sulphide treatment of germanium tetra-ethoxide, has been re-examined. It has been found that the reported X-ray diffraction pattern of the product previously obtained coincides with germanium dioxide and not disulphide. A repetition of the synthesis, and investigation of the product by infrared spectroscopy and X-ray diffractometry, shows that germanium disulphide is indeed formed but contamination by oxide is difficult to avoid.

    Original languageEnglish
    Pages (from-to)2599-2602
    Number of pages4
    JournalJournal of Materials Science
    Volume26
    Issue number10
    DOIs
    Publication statusPublished - 1 Jan 1991

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